GC-MS: Varian 450GC - 300 MS/MS
- Scan modes: Q1MS, Q3MS, Precursor (Parent), Product(Daughter), Neutral Loss, Selected Ion Monitoring (SIM), Selected Reaction Monitoring (SRM), Full Scan Ionization modes: Electron Ionization (EI) or positive/negative Chemical Ionization (CI)
- Source: EI/CI source with vacuum interlock for quick change of ion volumes; entrance hexapole isolates source contaminants from mass filter
- Source temperature: independent control, 20 C to 325 C
- Filament: single, 50 to 500 μA
- Electron energy: 20 eV, 70 eV or 150 eV
- Mass filters: quadruple with pre- and post-filters; lensless design maximizes transmission efficiency
- Collision cell: 180 curved path with pre- and post filter region; long path ensures high dissociation efficiency
- Mass range: up to 800 Da
- Scan rate: up to 6000 Da/sec
- Resolution: 0.7 Da at 1250 Da/sec or 0.6 Da at 500 Da/sec
- EI dynamic range: >10^5 (compound dependent)
- Mass axis stability: 0.1 Da over 24 hours
- Transfer line temperature: independent control; 50 C to 325 C
- Manifold temperature: independent control; 30 C to 50 C
- Ion detector: positive or negative ions, constant 5 kV post-acceleration voltage
- Carrier gas flow: up to 8 mL
Varian 450 GC
Column
FactorFour Capillary Column: VF-5ms, 30m x 0.25mm ID, DF=0.25um
Injectors
CP-1177 Split/Splitless Injector
- Temperature range: 50 C to 450 C isothermal
1079 PTV Injector
- Temperature range: -99 C to 450 C with LN2; -65 C to 450 C with LCO2
- Maximum temperature ramp rate: 200 C min
- Temperature ramps: 4
Injector EFC
- Pressure range: 0 to 100 psi
- Total flow: 500 mL/min at 10 psi
- QuickSwitch Valve: instantly switch between injector/ columns
- ChromatoProbe: probe device for solids, large volumes of liquids, or slurries