GC-MS: Varian 450GC - 300 MS/MS

  • Scan modes: Q1MS, Q3MS, Precursor (Parent), Product(Daughter), Neutral Loss, Selected Ion Monitoring (SIM), Selected Reaction Monitoring (SRM), Full Scan Ionization modes: Electron Ionization (EI) or positive/negative Chemical Ionization (CI)
  • Source: EI/CI source with vacuum interlock for quick change of ion volumes; entrance hexapole isolates source contaminants from mass filter
  • Source temperature: independent control, 20 C to 325 C
  • Filament: single, 50 to 500 μA
  • Electron energy: 20 eV, 70 eV or 150 eV
  • Mass filters: quadruple with pre- and post-filters; lensless design maximizes transmission efficiency
  • Collision cell: 180 curved path with pre- and post filter region; long path ensures high dissociation efficiency
  • Mass range: up to 800 Da
  • Scan rate: up to 6000 Da/sec
  • Resolution: 0.7 Da at 1250 Da/sec or 0.6 Da at 500 Da/sec
  • EI dynamic range: >10^5 (compound dependent)
  • Mass axis stability: 0.1 Da over 24 hours
  • Transfer line temperature: independent control; 50 C to 325 C
  • Manifold temperature: independent control; 30 C to 50 C
  • Ion detector: positive or negative ions, constant 5 kV post-acceleration voltage
  • Carrier gas flow: up to 8 mL

Varian 450 GC

Column 

FactorFour Capillary Column: VF-5ms, 30m x 0.25mm ID, DF=0.25um

Injectors

CP-1177 Split/Splitless Injector

  • Temperature range: 50 C to 450 C isothermal

1079 PTV Injector

  • Temperature range: -99 C to 450 C with LN2; -65 C to 450 C with LCO2
  • Maximum temperature ramp rate: 200 C min
  • Temperature ramps: 4

Injector EFC

  • Pressure range: 0 to 100 psi
  • Total flow: 500 mL/min at 10 psi
  • QuickSwitch Valve: instantly switch between injector/ columns
  • ChromatoProbe: probe device for solids, large volumes of liquids, or slurries